If you need to store a PicoFrit® Column*
for reuse on a later date, we recommend the use of a MicroTight® union,
fitting, and sleeves to protect the tapered end of the
column. Letting the column dry out for an extended period
of time may render it unuseable. Protecting the tip end
will allow you to store the column in a solvent-filled
vial, beaker, or centrifuge tube.
Slip the distal end of the PicoFrit® column
into the MicroTight® sleeve, and pull through.
DO NOT feed the column tip end first!
Pull the column further into the sleeve
so that the tip is fully covered and protected by the sleeve.
Tighten the fitting so that the column tubing is firmly
held in place.
Place the column into a suitable vial
or centrifuge tube and fill the container with suitable
mobile phase. (The same composition used for column conditioning
is recommended.) For best results, the column should be
vertical, with the tip pointed sown. For long-term storage,
the container should be covered with a suitable material
to retard solvent evaporation.
*This storage solution works only for
PicoFrit Columns without a conductive coating. Storing
coated tips and coated Self-Pack PicoFrit Columns in
the is manner will cause the platinum coating to separate
from the emitter tip.